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/*
* experiment.c
*
* Created: 01/10/2012 10:59:48 PM
* Author: mdryden
*/
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/**
* @file experiment.c
* @author Michael DM Dryden <mdryden@chem.utoronto.ca>
* @version 1.0
*
*
* @section DESCRIPTION
*
* Contains Functions for performing experiments and adjusting potentiostat settings other than DAC and ADC.
*/
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#include "experiment.h"
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//Public variable definitions
uint8_t g_gain = POT_GAIN_30k;
uint8_t autogain_enable = 1;
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//Private variables
volatile int32_t voltage = 0;
volatile uint16_t dacindex = 0;
uint16_t dacindex_stop = 0;
volatile int8_t up = 1;
volatile uint16_t iter = 0;
uint16_t* eis_ptr = 0;
volatile uint16_t cycles = 0;
volatile uint16_t samples = 0;
volatile uint16_t tcf0period = 0;
uint32_t skip_samples = 0;
//Private function declarations
static void porte_int0_lsv(void);
static void tcf0_ovf_callback(void);
static void tce1_ovf_callback_lsv(void);
static void lsv_cca_callback(void);
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static void ca_cca_callback(void);
static void portd_int0_ca(void);
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//interrupt callback setup
typedef void (*port_callback_t) (void);
static port_callback_t portd_int0_callback;
static port_callback_t portd_int1_callback;
void pot_init(void){
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/**
* Initializes AVR port directions and levels
*
* @return Nothing.
*/
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 1
arch_ioport_set_port_dir(IOPORT_PORTB, PIN3_bm|PIN4_bm|PIN5_bm|PIN6_bm|PIN7_bm, IOPORT_DIR_OUTPUT);
arch_ioport_set_port_dir(IOPORT_PORTD, PIN4_bm, IOPORT_DIR_OUTPUT);
arch_ioport_set_port_level(IOPORT_PORTB, PIN3_bm|PIN4_bm|PIN5_bm|PIN6_bm|PIN7_bm, PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
#endif
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 2
arch_ioport_set_port_dir(IOPORT_PORTB, PIN2_bm|PIN3_bm|PIN4_bm|PIN5_bm|PIN6_bm|PIN7_bm, IOPORT_DIR_OUTPUT);
arch_ioport_set_port_dir(IOPORT_PORTD, PIN4_bm, IOPORT_DIR_OUTPUT);
arch_ioport_set_port_level(IOPORT_PORTB, PIN2_bm|PIN3_bm|PIN4_bm|PIN5_bm|PIN6_bm|PIN7_bm, PIN3_bm|PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
#endif
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}
void pot_set_gain(void){
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/**
* Sets iV gain according to current g_gain value
*
* @return Nothing.
*/
switch (g_gain){
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 1
case POT_GAIN_500M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, 0);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
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case POT_GAIN_30M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 30M\n\r");
break;
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case POT_GAIN_3M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 3M\n\r");
break;
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case POT_GAIN_300k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 300k\n\r");
break;
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case POT_GAIN_30k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, 0);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 30k\n\r");
break;
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case POT_GAIN_3k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 3k\n\r");
break;
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case POT_GAIN_300:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 300\n\r");
break;
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case POT_GAIN_100:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 100\n\r");
break;
#endif
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 2
case POT_GAIN_100M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, 0);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 100M\n\r");
break;
case POT_GAIN_30M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 30M\n\r");
break;
case POT_GAIN_3M:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 3M\n\r");
break;
case POT_GAIN_300k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, 0);
printf("#INFO: 300k\n\r");
break;
case POT_GAIN_30k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, 0);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 30k\n\r");
break;
case POT_GAIN_3k:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 3k\n\r");
break;
case POT_GAIN_0:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 0\n\r");
break;
case POT_GAIN_100:
arch_ioport_set_port_level(IOPORT_PORTB, PIN6_bm|PIN7_bm, PIN6_bm|PIN7_bm);
arch_ioport_set_port_level(IOPORT_PORTD, PIN4_bm, PIN4_bm);
printf("#INFO: 100\n\r");
break;
#endif
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default:
printf("#WAR: Invalid pot gain.\n\r");
break;
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return;
}
}
void pot_exp_start(void){
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/**
* Connects measurement cell to rest of circuit.
*/
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 1
arch_ioport_set_port_level(IOPORT_PORTB, PIN3_bm|PIN4_bm|PIN5_bm, PIN3_bm|PIN4_bm|PIN5_bm);
#endif
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 2
arch_ioport_set_port_level(IOPORT_PORTB, PIN2_bm|PIN3_bm|PIN4_bm|PIN5_bm, PIN2_bm|PIN4_bm|PIN5_bm);
#endif
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}
void pot_exp_stop(void){
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/**
* Disconnects measurement cell and shorts RE and CE terminals.
*/
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 1
arch_ioport_set_port_level(IOPORT_PORTB, PIN3_bm|PIN4_bm|PIN5_bm, 0);
#endif
#if BOARD_VER_MAJOR == 1 && BOARD_VER_MINOR == 2
arch_ioport_set_port_level(IOPORT_PORTB, PIN2_bm|PIN3_bm|PIN4_bm|PIN5_bm, PIN3_bm);
#endif
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}
void cv_experiment(int16_t v1, int16_t v2, int16_t start, uint8_t scans, uint16_t slope){
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/**
* Perform a CV experiment.
*
* Calls lsv_experiment several times to make a CV experiment.
* @param v1 Vertex 1 in mV.
* @param v2 Vertex 2 in mV.
* @param start Start voltage in mV.
* @param scans Number of scans.
* @param slope Scan rate in mV/s.
*/
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// check if start is [v1,v2]
int8_t firstrun = 1;
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if((start < v1 && start < v2) || (start > v1 && start > v2)){
printf("#ERR: Start must be within [v1, v2]\n\r");
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return;
}
// RTC.CTRL = RTC_PRESCALER_OFF_gc;
// while (RTC.STATUS & RTC_SYNCBUSY_bm);
// RTC.CNT = 0;
// RTC.PER = 0xffff;
// RTC.CTRL = RTC_PRESCALER_DIV1024_gc; // 1 s tick
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while(scans > 0){
if (start != v1){
lsv_experiment(start,v1,slope,firstrun);
firstrun = 0;
}
if (start == v2 && scans == 1)
firstrun = -1;
lsv_experiment(v1,v2,slope,firstrun);
if (scans == 1)
firstrun = -1;
if (start != v2)
lsv_experiment(v2,start,slope,firstrun);
--scans;
firstrun = 0;
}
// printf("Time: %lu s \n\r", rtc_get_time());
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return;
}
void lsv_experiment(int16_t start, int16_t stop, uint16_t slope, int8_t first_run){
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/**
* Perform a LSV experiment.
*
* Uses porte_int0_lsv to output to USB.
* @param start Start potential in mV.
* @param stop Stop potential in mV.
* @param slope Scan rate in mV/s.
* @param first_run Keeps track of number of scans so potentiostat isn't initialized twice or disconnected when doing CV. Set to 2 for normal LSV.
*/
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//check experiment limits
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if(start<-1500 || start>=1500 ||start==stop|| stop<-1500 || stop>=1500 || slope>7000)
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{
printf("#ERR: Experiment parameters outside limits\n\r");
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return;
}
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uint16_t dacindex_start = ceil(start*(65536/(double)3000)+32768);
dacindex_stop = ceil(stop*(65536/(double)3000)+32768);
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// uint16_t period;
uint32_t timer_period;
uint16_t temp_div;
max5443_set_voltage1(dacindex_start);
if (first_run == 1 || first_run == 2){
pot_exp_start();
ads1255_rdatac();
tc_enable(&TCC1);
ads1255_sync();
tc_enable(&TCC0);
tc_set_overflow_interrupt_callback(&TCC0, tcf0_ovf_callback);
tc_set_overflow_interrupt_callback(&TCC1, tce1_ovf_callback_lsv);
tc_set_cca_interrupt_callback(&TCC1, lsv_cca_callback);
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portd_int0_callback = porte_int0_lsv; //ADC read
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//set EVCH0 event
EVSYS.CH0MUX = EVSYS_CHMUX_TCC0_OVF_gc;
EVSYS.CH0CTRL = 0;
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timer_period = ceil(1/((double)slope/(3000./65536))*(F_CPU));
temp_div = ceil(timer_period/65536.);
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if (temp_div <= 1)
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV1_gc);
else if (temp_div == 2){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV2_gc);
timer_period /= 2;
}
else if (temp_div <= 4){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV4_gc);
timer_period /= 4;
}
else if (temp_div <= 8){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV8_gc);
timer_period /= 8;
}
else if (temp_div <= 64){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV64_gc);
timer_period /= 64;
}
else if (temp_div <= 256){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV256_gc);
timer_period /= 256;
}
else if (temp_div <= 1024){
tc_write_clock_source(&TCC0,TC_CLKSEL_DIV1024_gc);
timer_period /= 1024;
}
else{
printf("ERR: Frequency/ADC rate is too low\n\r");
return;
}
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//printf("Period:%lu\n\r", timer_period);
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ads1255_wakeup();
tc_write_period(&TCC1, 0xffff);
tc_write_period(&TCC0, (uint16_t)timer_period);
}
TCC1.CNT = dacindex_start;
if (stop > start)
{
up = 1;
tc_set_direction(&TCC1, TC_UP);
}
else
{
up = -1;
tc_set_direction(&TCC1, TC_DOWN);
}
tc_write_cc(&TCC1, TC_CCA, dacindex_stop);
tc_enable_cc_channels(&TCC1, TC_CCAEN);
TCC0.CNT = 0;
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tc_set_cca_interrupt_level(&TCC1, TC_INT_LVL_HI); //Stop experiment
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tc_set_overflow_interrupt_level(&TCC0, TC_OVFINTLVL_LO_gc); //Set DAC
PORTD.INTCTRL = PORT_INT0LVL_MED_gc; //ADC read
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tc_write_clock_source(&TCC1, TC_CLKSEL_EVCH0_gc);
while (up != 0); //Experiment run with interrupts
if (first_run == -1 || first_run == 2)
{
tc_disable(&TCC0);
TCC0.CNT = 0x0;
tc_disable(&TCC1);
pot_exp_stop();
ads1255_standby();
}
return;
}
static void porte_int0_lsv(void){
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/**
* ISR for taking LSV measurements.
*/
int32_t result;
static uint16_t last_value = 0;
uint32_t current = TCC1.CNT;
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result = ads1255_read_fast24();
printf("%lu %ld\n\r", (current+last_value)>>1, result); //DAC value is average of current and last timer - approximation of center of averaging window
last_value = (uint16_t)current;
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return;
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}
static void tcf0_ovf_callback(void){
max5443_set_voltage1(TCC1.CNT);
}
static void tce1_ovf_callback_lsv(void){
PORTD.INTCTRL = PORT_INT0LVL_OFF_gc;
tc_set_overflow_interrupt_level(&TCC0, TC_OVFINTLVL_OFF_gc);
tc_set_overflow_interrupt_level(&TCC1, TC_OVFINTLVL_OFF_gc);
up = 0;
return;
}
static void lsv_cca_callback(void){
PORTD.INTCTRL = PORT_INT0LVL_OFF_gc;
tc_set_overflow_interrupt_level(&TCC0, TC_OVFINTLVL_OFF_gc);
tc_set_cca_interrupt_level(&TCC1, TC_INT_LVL_OFF);
up = 0;
return;
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}
void chronoamp(uint16_t steps, uint16_t step_dac[], uint16_t step_seconds[]){
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/**
* Performs a chronoamperometry experiment.
*
* @param steps Total number of steps.
* @param step_dac[] Array containing DAC indices.
* @param step_seconds[] Array containing step durations in seconds.
*/
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while (RTC.STATUS & RTC_SYNCBUSY_bm);
RTC.PER = 999;
while (RTC.STATUS & RTC_SYNCBUSY_bm);
RTC.CTRL = RTC_PRESCALER_DIV1_gc; //1ms tick
RTC.CNT = 0;
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EVSYS.CH0MUX = EVSYS_CHMUX_RTC_OVF_gc; //EV CH0 -- RTC overflow 1s
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portd_int0_callback = portd_int0_ca; //ADC interrupt
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tc_enable(&TCC0);
tc_set_cca_interrupt_callback(&TCC0, ca_cca_callback);
ads1255_rdatac();
ads1255_wakeup();
tc_write_period(&TCC0,0xffff);
tc_write_clock_source(&TCC0, TC_CLKSEL_EVCH0_gc);
tc_set_direction(&TCC0, TC_UP);
tc_enable_cc_channels(&TCC0, TC_CCAEN);
tc_set_cca_interrupt_level(&TCC0, TC_INT_LVL_HI);
TCC0.CNT = 0;
pot_exp_start();
for (uint8_t i = 0; i < steps; ++i)
{
up = 1;
tc_write_cc(&TCC0, TC_CCA, TCC0.CNT+step_seconds[i]-1);
RTC.CNT=0;
max5443_set_voltage1(step_dac[i]);
//PORTE.INTCTRL = PORT_INT0LVL_LO_gc;
PORTD.INTCTRL = PORT_INT0LVL_LO_gc;
while (up !=0);
}
tc_set_cca_interrupt_level(&TCC0, TC_INT_LVL_OFF);
tc_write_clock_source(&TCC0, TC_CLKSEL_OFF_gc);
tc_disable(&TCC0);
pot_exp_stop();
ads1255_standby();
return;
}
static void portd_int0_ca(void){
printf("%u.%.3u %ld\n\r", TCC0.CNT, RTC.CNT, ads1255_read_fast24());
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}
static void ca_cca_callback(void){
/**
* Interrupt handler for CA. Triggers when counter matches CC to stop potential step.
*
*/
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//PORTE.INTCTRL = PORT_INT0LVL_OFF_gc;
PORTD.INTCTRL = PORT_INT0LVL_OFF_gc;
up = 0;
return;
}
void swv_experiment(int16_t start, int16_t stop, uint16_t step, uint16_t pulse_height, uint16_t frequency){
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/**
* Perform a SWV experiment
*
* @param start Start voltage in mV.
* @param stop Stop voltage in mV.
* @param step Step voltage in mV.
* @param pulse_height Pulse amplitude in mV.
* @param frequency Frequency in Hz.
*/
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//check experiment limits
// if((start-pulse_height)<-1500 || (start+pulse_height)>(1500)|| start == stop || stop<-1500 || (stop+pulse_height)>1500 || step<1 || step>1500 || pulse_height > 1500 || pulse_height < 1)
// {
// printf("ERR: Experiment parameters outside limits\n\r");
// //return;
// }
int32_t forward = 0;
int32_t reverse = 0;
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// int32_t data_buffer;
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uint8_t direction;
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uint16_t dacindex_start = ceil((start)*(65536/(double)3000))+32768;
uint16_t dacindex_stop = ceil(stop*(65536/(double)3000))+32768;
uint16_t dacindex_step = ceil(step*(65536/(double)3000));
uint16_t dacindex_pulse_height = ceil(pulse_height*(65536/(double)3000));
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uint16_t dacindex = dacindex_start;
uint32_t period;
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// int16_t fgain = -1;
// int16_t rgain = -1;
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if (start < stop)
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direction = 1;
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else
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direction = 0;
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tc_enable(&TCF0);
frequency *= 2; //compensate for half-period triggers
//calculate time to ADC trigger
period = ceil((1/(double)frequency)*F_CPU);
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uint8_t temp_div = ceil((double)period/65536);
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if (temp_div == 1)
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV1_gc);
else if (temp_div == 2){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV2_gc);
period /= 2;
}
else if (temp_div <= 4){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV4_gc);
period /= 4;
}
else if (temp_div <= 8){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV8_gc);
period /= 8;
}
else if (temp_div <= 64){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV64_gc);
period /= 64;
}
else if (temp_div <= 256){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV256_gc);
period /= 256;
}
else if (temp_div <= 1024){
tc_write_clock_source(&TCF0,TC_CLKSEL_DIV1024_gc);
period /= 1024;
}
else{
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printf("#Frequency/ADC rate is too low\n\r");
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return;
}
tc_write_period(&TCF0, (uint16_t)period);
if (direction == 1)
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max5443_set_voltage1(dacindex+dacindex_pulse_height);
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else
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max5443_set_voltage1(dacindex-dacindex_pulse_height);
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ads1255_wakeup();
ads1255_rdatac();
ads1255_sync();
pot_exp_start();
TCF0.CNT = 0;
while (!tc_is_overflow(&TCF0));
ads1255_wakeup();
TCF0.CNT = 0;
while ((dacindex <= dacindex_stop && direction == 1) || (dacindex >= dacindex_stop && direction == 0)){
tc_clear_overflow(&TCF0);
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printf("%u %ld %ld\n\r", dacindex, forward, reverse); //data output
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// forward = 0;
// reverse = 0;
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while (!tc_is_overflow(&TCF0)){ //convert continuously until tc overflow - datum is last collected point
while (ioport_pin_is_low(IOPORT_CREATE_PIN(PORTD, 5))); //wait for next valid datum
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while (ioport_pin_is_high(IOPORT_CREATE_PIN(PORTD, 5)));
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forward = ads1255_read_fast24();
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}
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if (direction == 1) //switch voltage to other half of cycle
max5443_set_voltage1(dacindex-dacindex_pulse_height);
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else
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max5443_set_voltage1(dacindex+dacindex_pulse_height);
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tc_clear_overflow(&TCF0); //reset timer OVF
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if (direction == 1) //increment dacindex
dacindex += dacindex_step;
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else
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dacindex -= dacindex_step;
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while (!tc_is_overflow(&TCF0)){ //wait for tc overflow
while (ioport_pin_is_low(IOPORT_CREATE_PIN(PORTD, 5))); //wait for next valid datum
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while (ioport_pin_is_high(IOPORT_CREATE_PIN(PORTD, 5)));
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reverse = ads1255_read_fast24();
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}
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//at new dacindex
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if (direction == 1)
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max5443_set_voltage1(dacindex+dacindex_pulse_height);
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else
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max5443_set_voltage1(dacindex-dacindex_pulse_height);
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}
pot_exp_stop();
tc_write_clock_source(&TCF0, TC_CLKSEL_OFF_gc);
tc_disable(&TCF0);
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TCF0.CNT = 0;